METHOD OF PRODUCING MOLYBDENUM CATALYST FOR OLEFIN EPOXIDATION Russian patent published in 2017 - IPC B01J23/28 B01J37/00 C07D301/19 

Abstract RU 2633363 C1

FIELD: chemistry.

SUBSTANCE: method for producing a molybdenum catalyst for the olefin epoxidation is carried out by dissolving metal powdered molybdenum at 30-50°C in wastewater with a peroxide concentration of 0.25-1.10 mol/l, wastewater is formed by the co-production of styrene and propylene oxide in the aqueous washing phase of ethylbenzene oxide. The method is characterised in that the dissolution of molybdenum is carried out in the presence of a 35% solution of hydrogen peroxide and ethyl alcohol at a weight ratio of wastewater: Mo 1:(0.05-0.3), respectively, and wastewater: hydrogen peroxide: ethyl alcohol 1:(0.1-1):(10.4-65.3), respectively.

EFFECT: simplification of the method, since no dehydration and further dissolution of the catalyst in the hydrocarbon medium before the olefin epoxidation process is required.

2 tbl, 8 ex

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RU 2 633 363 C1

Authors

Kharlampidi Kharlampij Evklidovich

Gajfullin Anvar Akhmetovich

Elimanova Galina Gennadevna

Miroshkin Nikolaj Petrovich

Tuntseva Svetlana Nikolaevna

Dates

2017-10-12Published

2016-12-08Filed