METHOD OF PRODUCING COMPOSITE MATERIALS AS POLYMER MATRICES FILLED WITH NANOPARTICLES OF METAL OXIDES WITH MODIFIED SURFACE Russian patent published in 2017 - IPC C08J3/28 C08K13/06 C08K3/22 C08K5/19 C08L101/00 C08L27/06 B82B3/00 C08K5/98 C08L25/06 C08J5/18 

Abstract RU 2638658 C2

FIELD: chemistry.

SUBSTANCE: for the production of composite materials, the surface of the original BaTiO3 nanoparticles is preliminarily activated by the application of hydroxyl groups by boiling in a hydrogen peroxide solution and modified with cationic surfactant molecules by treatment with a solution of a cationic surfactant at a concentration below the critical micelle concentration. The resulting precipitate is filtered, washed from the cationic surfactant unbound to the surface of the metal oxide nanoparticles, and dried. The nanoparticles BaTiO3 with a modified surface are introduced into the polymer solution, achieving the desired volume ratio of the filler and the polymer matrix, and subjected to ultrasonic dispersion.

EFFECT: simplification of the method of producing composite materials in the form of polymer matrices filled with nanoparticles of oxide ferroelectrics with a modified surface, allowing to reduce the degree of aggregation of nanoparticles in the polymer.

3 dwg

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RU 2 638 658 C2

Authors

Emelyanov Nikita Aleksandrovich

Dates

2017-12-15Published

2015-09-02Filed