PROCESS FOR PREPARATION OF N-(2-HYDROXYETHYL)-O-ISOPROPYLCARBAMATE Russian patent published in 2018 - IPC C07C269/04 C07C271/16 

Abstract RU 2651792 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a process of obtaining of N-(2-hydroxyethyl)-O-isopropylcarbamate (Formula I), which is used as a plant growth regulator, and also increases their resistance to stress factors. According to the process of the invention, a reaction is carried out of diisopropyl carbonate obtained with isopropyl alcohol and triphosgene in the presence of pyridine used as an acceptor of hydrogen chloride, with monoethanolamine at 60–100 °C in presence of strong bases selected from sodium methylate, or sodium isopropylate, or potassium t-butoxide, or sodium butoxide.

.

EFFECT: proposed method is convenient, environmentally safe and allows to obtain the product in good yield and purity.

1 cl, 5 ex

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RU 2 651 792 C1

Authors

Nefedov Pavel Andreevich

Gordeev Dmitrij Alekseevich

Dashkin Ratmir Rinatovich

Mantrov Sergej Nikolaevich

Dates

2018-04-24Published

2016-12-23Filed