GEL WITH HIGH DEGREE OF DISPERSIBILITY AND METHOD OF ITS PRODUCTION Russian patent published in 2019 - IPC C01F7/14 C01F7/34 B01J13/00 B82B1/00 B82Y30/00 

Abstract RU 2694751 C2

FIELD: chemistry.

SUBSTANCE: invention can be used in chemical industry. Method of producing aluminium oxide gel involves a first step of depositing aluminium oxide, involving deposition of at least one basic precursor and at least one acidic precursor in an aqueous reaction medium. At least one of precursors - basic or acid - contains aluminium. Relative flow of acidic and basic precursors is selected so that pH of reaction medium is from 8.5 to 10.5. First stage of sedimentation is carried out at 10–50°C for 2–30 minutes. Then, suspension second stage is carried out by adding at least one basic precursor and at least one acidic precursor. Second deposition step is carried out at 40–90 °C for 2–50 minutes. Suspension is heated between the first and second deposition steps and after the second precipitation step. Further, the obtained suspension is thermally treated at 50–200 °C for a period of time of 30 minutes to 5 hours. Filtration step is then carried out with at least one washing step of the obtained gel.

EFFECT: invention enables to obtain aluminium oxide gel, characterized by improved filterability.

7 cl, 5 tbl, 5 ex

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RU 2 694 751 C2

Authors

Boualleg, Malika

Bouvry, Celine

Euzen, Patrick

Dates

2019-07-16Published

2015-06-09Filed