FIELD: chemistry.
SUBSTANCE: invention relates to production of mineral salts and fertilizers and can be used for production of potassium nitrate. Method of producing potassium nitrate involves converting a solution of a mixture of sodium nitrate with potassium chloride, where sodium nitrate is added to the solution of the initial mixture while heating. Obtained mixture is cooled for potassium nitrate crystallization and separated from recycled solution. After separation of potassium nitrate potassium chloride or mixture of potassium and sodium chlorides is added to solution. Solution is evaporated to form sodium chloride crystals and separated from the recycled solution. Reverse solution having molar ratio of Cl-:NO3- ions, equal to (10–40):(60–90), respectively, is directed to prepare initial mixture. Mass fraction of chloride-ion in the finished product – potassium nitrate crystals is 0.1–0.36 %.
EFFECT: method enables to obtain potassium nitrate with minimum content of chloride impurities.
1 cl, 1 dwg, 1 tbl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING POTASSIUM NITRATE AND MAGNESIUM CHLORIDE FROM POTASSIUM CHLORIDE AND MAGNESIUM NITRATE | 2008 |
|
RU2393117C1 |
METHOD OF PRODUCING POTASSIUM NITRATE | 2020 |
|
RU2739569C1 |
METHOD FOR PREPARING CALCIUM CHLORIDE AND POTASSIUM NITRATE FROM POTASSIUM CHLORIDE AND CALCIUM NITRATE | 2002 |
|
RU2206506C1 |
METHOD OF PRODUCING MAGNESIUM CHLORIDE AND CALCIUM NITRATE IN CLOSED CYCLE | 2008 |
|
RU2393118C1 |
METHOD FOR OBTAINING A MIXTURE OF ZIRCONIUM AND HAFNIUM NITRATE AND OXYNITRATE CRYSTALS | 2022 |
|
RU2780209C1 |
METHOD FOR PRODUCING POTASSIUM AND SODIUM CHLORIDES FROM POTASSIUM-SODIUM CONTAINING RAW MATERIALS | 2022 |
|
RU2792270C1 |
PROCESS FOR RECOVERING POTASSIUM CHLORIDE FROM SILVINITES | 0 |
|
SU1000397A1 |
METHOD OF OBTAINING CALCIUM FORMATE | 2017 |
|
RU2665469C1 |
METHOD OF DIAMMONIUM PHOSPHATE PRODUCTION | 2023 |
|
RU2807991C1 |
METHOD OF PREPARING POTASSIUM SULFATE | 1995 |
|
RU2144500C1 |
Authors
Dates
2019-11-12—Published
2019-04-23—Filed