FIELD: chemistry.
SUBSTANCE: invention relates to a method for producing para-tert-butylcumol (PTBC), which is used for producing polymers and copolymers for creating compositions of paints, coatings and thermosetting resins. The method consists in the alkylation of cumene with tert-butyl alcohol (TBA). Concentrated sulfuric acid is used as a catalyst, while it is added to the reaction mixture, maintaining the temperature at 10-25°C. Next, the process is carried out at a temperature of 10-35°C for 30-180 minutes at a molar ratio of cumene: TBA:H2SO4 - 3:1:3.
EFFECT: high yields of para-tert-butylcumene, which does not contain impurities of ortho- and meta-isomers.
1 cl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF OBTAINING PARA TERTIARY BUTYL PHENOL AND ACETONE | 2017 |
|
RU2680599C1 |
METHOD OF PRODUCING ETHYLENE POLYMERISATION CATALYSTS WITH 1-(4-TERT-BUTYLPHENYL)ETHYL MOIETY | 2024 |
|
RU2827710C1 |
METHOD FOR OBTAINING C-H-ACID (MET)ACRYLATES | 2019 |
|
RU2760893C1 |
METHOD FOR RACEMIC DIORGANOSILYL-BIS-(2-METHYLBENZO-[e]INDENYL)ZIRCONIUM COMPOUNDS DIASTEREOSELECTIVE SYNTHESIS, AND RACEMIC COMPOUND OF TRANSITION METAL | 2003 |
|
RU2337104C9 |
OBTAINING PARTIALLY HYDRATED ANSA-METALLOCENE COMPLEXES | 2003 |
|
RU2333215C2 |
PRODUCTION OF SUBSTITUTED PHENYLENE AROMATIC DIESTERS | 2009 |
|
RU2553475C2 |
METHOD OF PHENOL SYNTHESIS | 1989 |
|
RU2014318C1 |
METHOD OF SYNTHESIS OF 1,10-, 1,7- AND 4,7-PHENANTHROLINES | 1994 |
|
RU2117006C1 |
METHOD OF OBTAINING CUMOL | 0 |
|
SU622801A1 |
RACEMIC-SELECTIVE OBTAINING, YIELDING ANSA-METALLOCENE BIPHENOXIDE COMPLEXES, WITH RELATIVELY SHORT ISOMERISATION TIME | 2003 |
|
RU2329272C2 |
Authors
Dates
2021-06-11—Published
2020-07-21—Filed