FIELD: chemistry.
SUBSTANCE: invention relates to a method for the electrochemical preparation of a zinc(II) coordination compound involving the interaction of a metal ion with a ligand in a two-component solvent medium followed by separation of the precipitate. The method is characterized by the fact that the interaction of a metal ion with a ligand is carried out by electrolysis of a solution containing 2,3,4,5-tetrahydro-2-imino-4-oxo-1,3-thiazole-5-acetic acid and an equimolar amount of sodium hydroxide with zinc electrodes, while the mass ratio of water: ethanol: sodium hydroxide: 2,3,4,5-tetrahydro-2-imino-4-oxo-1,3-thiazole-5-acetic acid is 25.00:19.73:0.37:1.60, the density of direct electric current is 3-5 mA/cm2.
EFFECT: production of a zinc (II) coordination compound by electrochemical method in one stage and with less time.
1 cl, 4 dwg, 3 tbl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD FOR PRODUCING A COORDINATION COMPOUND OF COPPER(II) WITH 2,3,4,5-TETRAHYDRO-2-IMINO-4-OXO-1,3-THIAZOLE-5-ACETIC ACID | 2021 |
|
RU2774950C1 |
| METHOD FOR ELECTROCHEMICAL PRODUCTION OF COORDINATION COMPOUND OF ZINC (II) | 2024 |
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| THIAZOLBENZOHETEROCYCLES, METHODS OF THEIR SYNTHESIS, MEDICINAL AGENT, INTERMEDIATE SUBSTANCES FOR SYNTHESIS OF THIAZOLBENZOHETEROCYCLES | 1998 |
|
RU2198889C2 |
| METHOD OF OBTAINING THE COORDINATION CONNECTION OF ZINC WITH NICOTINE ACID | 2016 |
|
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| METHOD OF PRODUCING DERIVATIVES OF 1,5-BENZOTHIAZEPIN OR PHARMACEUTICALLY ACCEPTABLE SALTS THEREOF | 0 |
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SU1435152A3 |
| METHOD OF PRODUCING DERIVATIVES OF 1,5-BENZOTHIAZEPINE OR SALTS THEREOF WITH HYDROHALIC ACID | 0 |
|
SU1454252A3 |
| DERIVATIVES OF 1,5-BENZODIAZEPINE, METHOD OF THEIR SYNTHESIS, PHARMACEUTICAL COMPOSITION | 1993 |
|
RU2124009C1 |
| TETRAHYDROIMIDAZO-[1,4]-BENZODIAZEPINES OR THEIR PHARMACEUTICALLY ACCEPTABLE SALTS OR STEREOISOMERS, A METHOD OF THEIR SYNTHESIS, INTERMEDIATE COMPOUNDS FOR THEIR SYNTHESIS AND ANTIVIRAL COMPOSITION | 1992 |
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| CONDENSED BENZAZEPINE DERIVATIVE, AN INTERMEDIATE COMPOUND FOR ITS SYNTHESIS, A PHARMACEUTICAL COMPOSITION | 1994 |
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