FIELD: production of lithium-ion batteries.
SUBSTANCE: method for producing a cathode material of the composition Li3V2(PO4)3 includes hydrothermal treatment of the initial aqueous mixture of lithium carbonate, ammonium dihydrogen phosphate and vanadyl formate of the composition VO(HCOO)2⋅H2O, taken in a stoichiometric ratio. Hydrothermal treatment is carried out at a temperature of 180-200°C for 8-10 hours. The resulting product is dried in an argon or helium atmosphere until a constant weight is obtained and annealed in an argon or helium atmosphere at a temperature of 700-750°C for 4-5 hours.
EFFECT: invention makes it possible to obtain a pure cathode material of composition Li3V2(PO4)3 in a nanodispersed state.
1 cl, 2 dwg, 2 ex
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Authors
Dates
2023-08-08—Published
2023-01-11—Filed