FIELD: ceramics.
SUBSTANCE: invention relates to production of ceramic oxide materials and making elements of complex shape with given properties and can be used in devices of self-calibrating temperature sensors as a temperature element, as well as in electronics to expand the field of their application. Method of producing ceramic temperature reference based on Zn1−xNixFe2O4 ferrites of variable composition, where the initial raw material for producing ferrites, the synthesis of which is carried out by a solid-phase reaction, are oxides of nickel, zinc and iron (III). Oxides are ground for 20 minutes, then the mixture is pressed under pressure of 30 kg/mm2. Produced pellet is subjected to synthesizing firing at temperature of 1,400 °C for 5 hours, adding 5 wt.% paraffin, as well as gasoline, heating to 100–150 °C until complete dissolution of paraffin. Article is sintered at temperature of 1,400 °C for an hour.
EFFECT: invention enables to obtain ferrite ceramics in the form of a monolithic article of complex geometric shape with high magnetic permeability.
3 cl, 3 dwg, 4 tbl
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Authors
Dates
2024-08-19—Published
2023-11-30—Filed