METHOD OF PRODUCING POROUS MATERIAL BASED ON SOLUTION OF COLLAGEN HYDRATE OF FRESHWATER HYDROBIONTS AND POLYVINYLPYRROLIDONE Russian patent published in 2025 - IPC C08H1/06 C07K1/14 C07K14/78 C12P21/06 B01D11/02 

Abstract RU 2832909 C1

FIELD: biotechnological industry.

SUBSTANCE: invention relates to a method of producing a porous material with sorption capacity with respect to components of heated glycerine aerosols. Method for producing a porous material based on a solution of collagen hydrate of freshwater hydrobionts and polyvinylpyrrolidone (PVP) involves acceptance of skin of freshwater scaleless fish, cleaning them from muscle tissue, fins and mechanical impurities, primary washing is carried out in water at ratio of 1 wt % solution of food surfactant: raw material—2 l of solution: 1 kg of raw material with mechanical mixing in a drum-type system with a drum rotation frequency of not less than 400 rpm at room temperature for 30 minutes, and then washing with water until complete removal of surfactant, maintenance of dermal covers in peroxide-alkaline solution containing 750 mM sodium hydroxide and 300 mM hydrogen peroxide, at room temperature until skin decolouration at the ratio of solution: raw material—2.5 l of solution: 1 kg of raw material, respectively, subsequent washing of treated dermal covers of freshwater hydrobionts with running water at temperature of 12±1 °C until complete removal of acid and alkali at weight ratio of dermal integuments: water—1:3, respectively, with constant stirring, operation is repeated three times, holding with constant stirring for 10 minutes at each stage, subsequent exposure of the washed skins in a weak organic acid solution is carried out at pH 4 for 48 hours and constant exposure to ultrasound with frequency of 100 kHz, holding the washed hides in a solution of a weak organic acid at pH 4 and constant exposure to ultrasound with frequency of 100 kHz is carried out in a weight ratio of the hide to the weak organic acid—1:3, and then the liquid phase is removed by draining, distilled water is added to the obtained semi-product at a weight ratio of semi-product: water—1:3, respectively, homogenisation is carried out using a blade-type homogenizer with power of 400 W for 5 minutes with a blade rotation frequency of 600 rpm until a dispersion is obtained, obtained dispersion is filtered using a filter with pore diameter of 0.45 mcm, the obtained substance is mixed with PVP in mass ratio of semi-product: PVP—1:1, respectively, substance is lyophilized at pressure of 3.3 Pa and a temperature of −44.5±1 °C for 18 hours to a residual moisture content in substance of 4%, obtained porous material is cut into plates and subjected to cold sterilization using ultraviolet radiation, vacuum packed.

EFFECT: obtained porous material according to the above method reduces content of components of heated glycerine aerosol.

1 cl, 2 dwg, 3 ex

Similar patents RU2832909C1

Title Year Author Number
FRESHWATER HYDROBIONT COLLAGEN HYDRATE SOLUTION PREPARATION METHOD 2021
  • Antipov Sergej Sergeevich
  • Artyukhov Valerij Grigorevich
  • Antipova Lyudmila Vasilevna
  • Yazykov Aleksandr Yurevich
RU2789758C1
METHOD FOR OBTAINING A POROUS MOISTURE ABSORBENCY MATERIAL ON A COLLAGEN BASIS 2021
  • Kotov Ivan Ivanovich
  • Antipova Lyudmila Vasilevna
RU2760326C1
METHOD OF PRODUCING POROUS COLLAGEN MATERIAL 2018
  • Antipova Lyudmila Vasilevna
  • Storublevtsev Stanislav Andreevich
  • Piskova Marina Aleksandrovna
  • Sukhov Igor Viktorovich
RU2704248C1
METHOD FOR PRODUCTION OF ACETIC DISPERSION OF HIGH MOLECULAR FISH COLLAGEN 2014
  • Semenycheva Ljudmila Leonidovna
  • Astanina Margarita Viktorovna
  • Kuznetsova Julija Leonidovna
  • Valetova Natal'Ja Borisovna
  • Geras'Kina Evgenija Viktorovna
  • Tarankova Ol'Ga Aleksandrovna
RU2567171C1
METHOD FOR PREPARATION OF COLLAGEN PRODUCT 2014
  • Antipova Lyudmila Vasilevna
  • Storublevtsev Stanislav Andreevich
  • Bolgova Svetlana Borisovna
RU2614273C2
METHOD TO PRODUCE TANNED HALF STUFF FROM SKIN OF ALL KINDS OF FRESH-WATER FISH 2009
  • Antipova Ljudmila Vasil'Evna
  • Dvorjaninova Ol'Ga Pavlovna
  • Bukaj Galina Aleksandrovna
  • Chudinova Ljubov' Petrovna
RU2425893C2
METHOD FOR PRODUCING HIGH-MOLECULAR COLLAGEN 2020
  • Khitrov Anatolij Anatolevich
  • Basarygin Artem Sergeevich
RU2746215C1
METHOD FOR PRODUCTION OF LEATHER SEMI-PRODUCT OF ALL TYPES OF FRESHWATER FISH 2018
  • Antipova Lyudmila Vasilevna
  • Kaverina Viktoriya Yurevna
RU2704442C1
METHOD FOR PRODUCING COLLAGEN BASE WITH ASEPTIC PROPERTIES 2020
  • Antipova Lyudmila Vasilevna
  • Storublevtsev Stanislav Andreevich
RU2739396C1
METHOD FOR PRODUCTION OF NATIVE COLLAGEN PRODUCT 2020
  • Ogarkov Eduard Vladimirovich
  • Sorokina Natalia Iurevna
RU2789021C2

RU 2 832 909 C1

Authors

Antipov Sergej Sergeevich

Vandyshev Dmitrij Yurevich

Kuchmenko Tatyana Anatolevna

Artyukhov Valerij Grigorevich

Dates

2025-01-09Published

2023-12-28Filed