FIELD: organic chemistry. SUBSTANCE: synthesis is carried out from 1-trifluoroacetylaminonaphthalene-5-sulfochloride and aqueous solution of NH7OH following by extraction with ethylacetate or acetone. Yield, % ; m. p. C; gross-formula: Ia) 90; 172; C12H15BrN2O2S; Ib) 83; 125-127; C12H14N2O2S; 1c) 86; 164-166; C16H2BrN2O2S. Method ensures to assay multi-components mixture of proteases. EFFECT: enhanced yields of products, selectivity of detected groups splitting off. 2 tbl
Authors
Dates
1994-03-15—Published
1987-04-17—Filed