FIELD: industry of synthetic rubber. SUBSTANCE: method involves polymerization of butadiene-1,3 in the medium of hydrocarbon solvent containing water in the presence of catalyst, which consists of cobalt salt and alkylaluminium chloride. Components of catalyst are added in 4.9-100% of initial volume of butadiene-1,3 solution, which is cooled up to (-10)-(-20) C. Residual quantity of cooled solution is added then to the mixture, and temperature is increased up to 20-30 C. EFFECT: improved method of preparing. 1 tbl
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Authors
Dates
1994-04-30—Published
1992-12-23—Filed