FIELD: organic chemistry. SUBSTANCE: product of the formula R1-Si(R2)2-Si(R2)2-R1 , where R1 and R2 - are similar or different alkyls; conversion is 98.0%. Reagent 1: R1Cl2Si-SiCl2R2. Reagent 2: R2MgCl. Reaction conditions: in toluene medium with ethylated vat waste of methylchlorosilanes direct synthesis at their mass ratio (1:1)-(1:2) in the presence of ethyl ether. EFFECT: improved method of synthesis. 2 cl, 2 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF SYNTHESIS OF ETHYL-SUBSTITUTED SILANE MIXTURE | 1992 |
|
RU2035464C1 |
METHOD FOR PRODUCTION OF MONOMERS WHICH CONTAIN FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLENE SILOXANE LIQUIDS | 1992 |
|
RU2061697C1 |
METHOD OF SYNTHESIS OF PHENYLETHOXYSILANES | 1992 |
|
RU2053233C1 |
METHOD OF ORGANOALKOXYSILANES SYNTHESIS | 1989 |
|
SU1626654A1 |
PROCESS FOR PREPARING MIXTURE OF ETHYL-SUBSTITUTED SILANES | 1989 |
|
SU1626653A1 |
METHOD FOR SYNTHESIS OF ORGANOALKOXY- AND CHLOROSILANES, AND APPARATUS FOR ITS REALIZATION | 0 |
|
SU1768605A1 |
METHOD OF PREPARING POLYPHENYL SILOXANES | 1992 |
|
RU2034866C1 |
METHOD OF PREPARING OF POLYETHYLSILOXANE LIQUIDS | 1992 |
|
RU2034864C1 |
METHOD OF PRODUCING POLYETHYLENESILOXANE FLUIDS | 0 |
|
SU1657514A1 |
PROCESS FOR PREPARING MONOMERS CONTAINING FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLSILOXANE LIQUIDS | 1989 |
|
SU1621466A1 |
Authors
Dates
1995-05-20—Published
1992-08-26—Filed