FIELD: organic chemistry. SUBSTANCE: product: mixture of phenylethoxysilanes of the following composition, wt.-%: PhH, PhCl, (Ph)2, Si(OEt)4, Ph2Si(OEf)3: 1.6-1.8; 0.7-5.9; 0.7-0.9; 39-49; 21-27; 7-13. Reagent 1: Mg. Reagent 2: C6H5Cl. Reagent 3: (C2H5O)4Si, vat waste of direct synthesis of methylchlorosilanes. Reaction conditions: 3-75 molar excess of Mg and countercurrent feeding reagents and magnesium. EFFECT: improved method of synthesis. 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING POLYPHENYL SILOXANES | 1992 |
|
RU2034866C1 |
METHOD FOR PRODUCTION OF PHENYL ETHOXYSILANES | 1992 |
|
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PROCESS FOR PREPARING PHENYLETHOXY SILANES | 1993 |
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PROCESS FOR PREPARING MIXTURE OF ETHYL-SUBSTITUTED SILANES | 1989 |
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METHOD FOR PRODUCTION OF MONOMERS WHICH CONTAIN FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLENE SILOXANE LIQUIDS | 1992 |
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RU2061697C1 |
METHOD OF CHLORO-CONTAINING MIXTURE PROCESSING | 1992 |
|
RU2068848C1 |
METHOD FOR PRODUCTION OF ORGANOALKOXY SILANES | 1993 |
|
RU2079502C1 |
Authors
Dates
1996-01-27—Published
1992-08-26—Filed