FIELD: chemical technology. SUBSTANCE: trichlorosilane is synthesized by interaction of silicon tetrachloride with technical silicon and hydrogen chloride at 380-450 C following by separation of chlorosilanes mixture on the diffusion diaphragms. Synthesized trichlorosilane contains SiCl46·10-2 vol. metal impurities are less 1·10-6 wt.-% Method is used for synthesis trichlorosilane of high-quality. EFFECT: improved method of synthesis, enhanced quality of product.
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Authors
Dates
1995-06-27—Published
1993-04-16—Filed