FIELD: organic chemistry. SUBSTANCE: product: 7-acetyl-6-methoxy-3-methyl-1-phenyl-1H-1,2-diazaphenalene of the formula (I) 
, empirical formula is C21H18N2O2, yield is 70% m. p. is 118 C. Reagent 1: 6-methoxy-3-methyl-1-phenyl-1H-1,2-diazaphenalene. Reagent 2: Wilsmeier reagent POCl + CH-C(O)N(CH). Reaction conditions: heating at 85-90 C for 30 min. Synthesized compound is used in pharmaceutical chemistry. EFFECT: improved method of synthesis.
| Title | Year | Author | Number |
|---|---|---|---|
| 1-BENZYL-6-METHOXY-3-METHYL-1H-1,2-DIAZAPHENALENE HAVING HYPOTENSIVE ACTIVITY | 1989 |
|
SU1623143A1 |
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|
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SU1607348A1 |
