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2 066 563

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C1

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IPC

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Application

95110306/04, 1995-06-21

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Actual filing date

1995-06-21

(45)

Published

1996-09-20

(72)

Inventor

Jakushkin M.I.Batrin Ju.D.Nikolaev Ju.T.Makarovskij I.A.Golovachev V.A.Starovojtov M.K.Fokin N.S.Gajdin L.I.Trofimchenko S.M.Beljakov N.G.

(73)

Holder

Jakushkin Mikhail IvanovichBatrin Jurij DmitrievichNikolaev Jurij Timofeevich

CATALYST FOR N-METHYLANILINE SYNTHESIS Russian patent published in 1996 - IPC

Abstract RU 2066563 C1

FIELD: catalytic chemistry, chemical technology. SUBSTANCE: invention relates to petrochemical synthesis, catalysts for synthesis of N-alkylated aromatic amines in the presence of hydrogen. Proposed catalyst has the following composition, wt.-%: copper oxide 9-15; manganese oxide 2.0-2.9; aluminium oxide - the rest for N-alkylation of aniline with methanol in the presence of hydrogen at 220-270 C. Proposed catalyst ensures to carry out N-alkylation of aniline with methanol at aniline conversion up to 98.8%, yield of N-methylaniline is 96.3%. Catalyst retains activity for 3000 hr without regeneration. EFFECT: enhanced effectiveness and quality of catalyst.

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RU 2 066 563 C1

Authors

Jakushkin M.I.

Batrin Ju.D.

Nikolaev Ju.T.

Makarovskij I.A.

Golovachev V.A.

Starovojtov M.K.

Fokin N.S.

Gajdin L.I.

Trofimchenko S.M.

Beljakov N.G.

Dates

1996-09-20—Published

1995-06-21—Filed

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