FIELD: organic chemistry, namely, method for production of dihydrate of 3-(2,2,2-trimethyl hydrazinium)propionate which may be used in medicine and in agriculture. SUBSTANCE: method involves alkaline hydrolysis of iodide-, or bromide-, or chloride of trimethylsilyl ester of 3-(2,2,2-trimethyl hydrazinium) propionic acid. The process takes place at room temperature at pH 8.0-8.5 according to given scheme wherein X= Br, J, Cl. Yield of desired dihydrate of 3-(2,2,2-trimethyl hydrazinium)propionate is 90-96 %. EFFECT: improved efficiency of the method.
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0 |
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Authors
Dates
1998-07-10—Published
1995-10-26—Filed