FIELD: crystal growing. SUBSTANCE: when preparing potassium titanyl arsenate monocrystals useful in laser technology as laser emission frequency converter, as inoculate for cooled solution-melt from intrinsic arsenate fluxes in K2O-TiO2-As2O5 system, melt with molar ratio of solvent components K2O:As2O5 from 0.8:1 to 2.2:1 supplemented with 1 to 10 mol % alkali-earth metal oxide (Mg, Ca, Sr or Ba oxide) is used and crystal is grown by cooling solution and simultaneously pulling inoculate oriented in direction [100] or [010] or normally to crystal plane [011]. EFFECT: enabled preparation of defect-free monocrystals 30x40x40 cu.mm in size and weight up to 70 g. 4 ex
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Authors
Dates
1999-04-10—Published
1997-02-17—Filed