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2 135 455

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IPC

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Application

98103113/04, 1998-02-23

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Start date

1998-02-23

(22)

Actual filing date

1998-02-23

(45)

Published

1999-08-27

(72)

Inventor

Dzhemilev U.M.Khusnutdinov R.I.Parfenova R.I.Atnabaeva A.M.Muslimov Z.S.

(73)

Holder

Institut Neftekhimii I Kataliza An Rb

METHOD OF SYNTHESIS OF 10-HYDROXYHEXACYCLO-[9.2.1.0.0.0,57,0]=TETRADECANE (HEXACYCLOTETRADECANOL-10) Russian patent published in 1999 - IPC

Abstract RU 2135455 C1

FIELD: organic chemistry. SUBSTANCE: 10-hydroxyhexacyclo-[9.2.1.02,6.03,8.0,57,09,13]-tetradecane (hexacyclo- -tetradecanol-10) is synthesized by interaction of norbornadiene dimer (binor-S) with water in the presence of palladium-containing catalyst in medium containing a solvent and water at ratio = (12-17):(3-1) at 180 C for 7 h. Regeneration of water and ether provides process occurring with formation of minimal amount of sewage and waste. EFFECT: improved and simplified method of synthesis. 1 tbl, 14 ex

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RU 2 135 455 C1

Authors

Dzhemilev U.M.

Khusnutdinov R.I.

Parfenova R.I.

Atnabaeva A.M.

Muslimov Z.S.

Dates

1999-08-27—Published

1998-02-23—Filed

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