METHOD OF PREPARING 5,5'-(OXYDI)PENTAN-2-ONE Russian patent published in 2003 - IPC

Abstract RU 2197466 C2

FIELD: organic synthesis. SUBSTANCE: invention relates to preparation of 5,5'-(oxydi)pentan-2-one, which can be used as multifunctional solvent, extractant, fragrance compound, and as raw material for synthesis of heterocyclic compounds. Method consists in reaction of acetylcyclopropane with water in diethyl ether medium in presence of copper-containing catalyst, in particular CuCl2•H2O or CuBr2 at acetylcyclopropane/catalyst/water molar ratio 1:(0.005-0,01):5 and temperature 180-200 C. Reaction time 6-10 h, yield of product 50-64%. EFFECT: enlarged assortment of various-destination organics. 1 tbl, 4 ex

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RU 2 197 466 C2

Authors

Atnabaeva A.M.

Parfenova R.I.

Muslimov Z.S.

Khusnutdinov R.I.

Dzhemilev U.M.

Dates

2003-01-27Published

2000-06-02Filed