FIELD: technology of preparation of benzoic acid. SUBSTANCE: described is preparation of benzoic acid by hydrolysis of methyl ester thereof. Neutralization of the resulting sodium benzoate is carried out with aqueous hydrochloric acid solution. Crystallization is carried out from solution containing 7-13% of benzoic acid and does not exceed 1 deg per minute during crystallization period. EFFECT: increased yield of the desired product. 4 ex
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Authors
Dates
2000-08-27—Published
1999-04-27—Filed