FIELD: inorganic compounds technologies. SUBSTANCE: invention, in particular, relates to monosilane appropriate for manufacturing especially pure semiconductor silicon. Method is characterized by that silicon tetrachloride is interacted with lithium hydride whose surface is subjected to activation with vibrating conveyer. Silicon tetrachloride gas flow is fed in counter-current mode into moving conveyer charged by lithium hydride and process is carried out at 290-300 C. EFFECT: increased yield of monosilane at lower temperature and reduced reaction time, enabled wasteless technology. 2 ex
Title | Year | Author | Number |
---|---|---|---|
PLANT FOR PRODUCTION OF MONOSILANE | 1999 |
|
RU2164218C1 |
METHOD OF PREPARING MONOSILANE | 1995 |
|
RU2077483C1 |
METHOD FOR PRODUCTION OF SILANES | 2003 |
|
RU2245299C2 |
METHOD OF SYNTHESIS OF SILANE | 2001 |
|
RU2194009C1 |
METHOD OF SYNTHESIS OF SILANE | 2001 |
|
RU2194010C1 |
METHOD OF PRODUCING POLYCRYSTALLINE SILICON IN CLOSED CIRCUIT | 1997 |
|
RU2122971C1 |
METHOD FOR CATALYTIC HYDROGENATION OF SILICON TETRACHLORIDE | 2011 |
|
RU2472704C1 |
METHOD OF PRODUCING SILICON CARBIDE LAYERS | 1993 |
|
RU2087416C1 |
SILANE PRODUCTION PROCESS | 2004 |
|
RU2267459C2 |
METHOD OF GRANULATION OF LITHIUM SALTS | 1998 |
|
RU2139247C1 |
Authors
Dates
2001-09-10—Published
1999-03-10—Filed