FIELD: chemical engineering. SUBSTANCE: method consists in selective isolation of hydrogen or its isotope via catalytic oxidation of hydrogen or its isotope with gaseous oxygen in presence of palladium-containing catalyst on inert carrier completed by ground metal appropriate for carrier metal. Reactor is heated under isothermal conditions, after which reactor is operated under autothermal. Regenerated gaseous waste is transferred into additional chamber. EFFECT: improved environmental safety of process and eliminated blast risk. 4 cl, 1 tbl, 3 ex
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