FIELD: industrial inorganic synthesis. SUBSTANCE: selenium is prepared via hydrogen reduction of selenium hexachloride in glow electric discharge at pressure (4-6)•102 Pa and selenium hexachloride-to-hydrogen molar ratio 1: (5-6.5). After washing and drying selenium product meets state standard requirements. EFFECT: improved purity and increased yield of product. 3 cl, 6 ex
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Authors
Dates
2004-02-27—Published
2002-04-10—Filed