FIELD: chemical technology, inorganic chemistry. SUBSTANCE: method involves interaction of selenium hexafluoride with reducing reagent: with 25-30% hydrazine hydrate aqueous solution at mass ratio selenium hexafluoride and hydrazine hydrate solution = 1:(10-14), acidification of the prepared mixture with hydrochloric acid to pH = 1-3, keeping the acidified mixture at 60-90 C for 1-1.5 h and isolation of the end product from its. Yield of the end product is 99.6-99.8% of theoretical value. EFFECT: increased yield of the end product. 4 cl
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Authors
Dates
1997-04-27—Published
1994-05-23—Filed