FIELD: crystal growing.
SUBSTANCE: method comprises growing germanium monocrystals from melt onto seed followed by heat treatment, the latter being effected without removing monocrystals from growing apparatus at temperature within 1140 and 1200 K during 60-100 h, temperature field being radially directed with temperature gradient 3.0 to 12.0 K/cm. Once heat treatment comes to end, monocrystals are cooled to 730-750°C at a rate of at most 60-80 K/h. Monocrystals are characterized by emission scattering at wavelength 10.6 μm not larger than 2.0-3.0% and extinction not higher than 0.02-0.03 cm-1, which is appropriate for use of monocrystals in IR optics.
EFFECT: allowed growth of germanium monocrystals with high optical characteristics.
3 ex
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Authors
Dates
2005-09-27—Published
2004-04-22—Filed