FIELD: medical devices, namely processes for forming coatings on surfaces of implants made of titanium in recrystallized or nano-structure state.
SUBSTANCE: coating contains, mass %: calcium titanate, 7 - 9; titanium pyrophosphate, 16 - 28; calcium phosphate compounds, the balance. Method comprises steps of anodizing implant by pulse electric current at condition of electric-spark discharge in phosphoric acid solution containing hydroxyapatite and calcium carbonate. Anodizing is realized by means of pulse current with next parameters: pulse time period, 50 - 200 ms; pulse repetition frequency 50 - 100 Hz; initial electric current density, 0.2 - 0.25 A/mm2; final voltage 100 -300 V. Invention allows to receive coating with thickness 40 - 80 micrometers.
EFFECT: possibility for forming coating whose composition is similar to that of osseous tissue with high content of calcium, improved osteoinductive and mechanical properties of coating.
7 cl, 3 ex
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Authors
Dates
2007-01-20—Published
2005-05-31—Filed