METHOD FOR MANUFACTURING POROUS-METAL CATHODES FROM TUNGSTEN POWDER Russian patent published in 2007 - IPC H01J9/04 

Abstract RU 2297068 C2

FIELD: electrical engineering; manufacturing porous-metal cathodes for electronic devices.

SUBSTANCE: proposed method for manufacturing porous-metal cathodes from tungsten powder includes step-by-step annealing of source powder at temperature ranging between 1650 and 1750 °C and raised by 25 - 50 °C, crushing of mold, quality control of powder after each annealing step by manufacturing specimen pellet compressed at constant pressure, and measurement of pressure P of air flowing through specimen pellet at P ≤ 0.45 kg/cm2 after second annealing stage, these being values of its open void channel in terms of air pressure, compression of pellets from powder obtained, their sintering in acid-free medium, and impregnation of sintered pellets with emission-active material; decision is taken to determine size of void channel till sintering for other pressure value for compression of specimen pellet, construction of calibration line P = f(Psp), determination of difference between void channel size in sintered and original state using reference curve showing this difference as function of sintering temperature Δ = f(Tsn); compression pressure is chosen from calibration line including reference dependence to obtain desired size of void channel in sintered pellets in terms of air flow pressure Psn max - Psn max by its values in non-sintered pellet within interval of (Psn min - Δ) - (Psn max - Δ), where Δ is difference in sizes of void channel in sintered and original states found from reference dependence; Psn is largest of open void channels out of set of tungsten frame void channels.

EFFECT: enhanced service life of cathodes and reduced degree of evaporation from them.

1 cl, 3 dwg, 3 tbl

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RU 2 297 068 C2

Authors

Usanov Dmitrij Aleksandrovich

Mel'Nikova Iraida Prokop'Evna

Mullin Viktor Valentinovich

Semenov Vladimir Konstantinovich

Kazakov Vladimir Konstantinovich

Najdenov Gennadij Petrovich

Dates

2007-04-10Published

2005-05-16Filed