FIELD: organic chemistry, chemical technology.
SUBSTANCE: invention relates to a method for synthesis of alkoxysilanes. Invention describes a method for synthesis of alkoxysilanes of the general formula: R'nSi(OR)m wherein n = 0-3; m = 1-4 and n + m = 4. Method involves reaction of chlorosilanes of the general formula: R'nSiClm wherein R' means hydrogen atom (H), CH3, C2H4, C2H or C6H6 with alcohols of the general formula: ROH wherein R means (C2-C8)-alkyl or (C2-C8)-aryl. Chlorosilane solution in an inert volatile nonpolar solvent is added to boiling alcohol solution in the same solvent at temperature 75-95°C, solvent is distilled off and evolving dry hydrogen chloride is captured. Method provides increasing yield, simplified process and decreasing time during the reaction carrying out.
EFFECT: improved method of synthesis.
6 cl, 1 tbl, 11 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING ALKOXYSILANES | 2009 |
|
RU2417228C1 |
METHOD OF OBTAINING FINE SILICA | 2010 |
|
RU2447020C1 |
METHOD OF PRODUCING POLYORGANOSILOXANES BASED ON ORGANOALKOXYSILANES | 2009 |
|
RU2428438C2 |
FIREPROOFING LACQUER | 2005 |
|
RU2299229C2 |
METHOD OF PRODUCING LINEAR POLY(METHYL)(HYDRIDE)SILOXANES WITH A GIVEN AVERAGE LENGTH OF A SILOXANE CHAIN | 2019 |
|
RU2712931C1 |
METHOD OF OBTAINING OLIGOORGANOSILOXANES | 2014 |
|
RU2556639C1 |
METHOD OF PRODUCING POLY(ORGANO)(ALKOXY)(HYDROXY)SILOXANES WITH GIVEN DEGREE OF POLYCONDENSATION | 2013 |
|
RU2524342C1 |
METHOD FOR OBTAINING CARBON FIBRE AND MATERIALS ON ITS BASIS | 2008 |
|
RU2384657C2 |
METHOD OF SYNTHESIS OF ALKOXYSILANES | 1998 |
|
RU2196142C2 |
METHOD OF PRODUCING POLYHEDRAL ORGANOSILSESQUIOXANES | 2010 |
|
RU2444539C1 |
Authors
Dates
2007-05-20—Published
2005-12-27—Filed