METHOD OF FORMING DIAMOND-STRUCTURED PARTICLES Russian patent published in 2007 - IPC C30B29/04 C30B25/10 C30B30/08 C23C16/26 

Abstract RU 2312175 C2

FIELD: carbon particles.

SUBSTANCE: invention relates to technology of preparing particles having monocrystalline diamond structure via growing from vapor phase under plasma conditions. Method comprises step ensuring functioning of plasma chamber containing chemically active gas and at least one carbon compound and formation of reactive plasma, which initiate appearance of seed particles in the plasma chamber. These particles ensure multidirectional growing of diamond-structured carbon thereon so that particles containing growing diamond are formed. Functioning of plasma chamber proceeds under imponderability conditions but can also proceed under gravitation conditions. In latter case, seed particles and/or diamond-containing particles in reactive plasma are supported under effect of external gravitation-compensating forces, in particular by thermophoretic and/or optic forces. Temperature of electrons in the plasma are lowered by effecting control within the range from 0.09 to 3 ev. Chamber incorporates plasma generator to generate plasma with reduced electron temperature and device for controlling forces to compensate gravitation and to allow particles to levitate in the plasma with reduced electron temperature. This device comprises at least one levitation electrode for thermophoretic levitation of particles in plasma with reduced electron temperature or an optical forceps device.

EFFECT: enabled efficient growing of high-purity duly shaped particles with monocrystalline diamond structure having sizes from 50 μm to cm range (for instance, 3 cm).

19 cl, 5 dwg

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RU 2 312 175 C2

Authors

Doze Fol'Ker

Morfill' Gregor

Fortov Vladimir Evgen'Evich

Sato Noriesi

Vatanabe Jukio

Tomas Khubertus M.

Dates

2007-12-10Published

2002-11-22Filed