METHOD FOR PREPARING 3-CHLOROPROPYLSILANE Russian patent published in 2008 - IPC C07F7/12 

Abstract RU 2320667 C1

FIELD: organic chemistry, chemical technology.

SUBSTANCE: invention relates to methods for synthesis of (-γ)-propylsilanes substituted at position 3. Invention proposes initial charging a platinum-containing catalyst and 10-30 wt.-% of reaction mass from previous step or vat residues after isolation of the end product from previous step into reactor. Then the mixture is heated to temperature 65°C and silane hydride and allyl chloride are dosed maintaining the mole ratio silane hydride and allyl chloride in the reaction mass = (1.0-1.2):1. Invention provides development of method allowing significant decreasing consumption of catalyst, declining formation of by-side products and enhancing the effectiveness of technological process.

EFFECT: improved method of synthesis.

3 cl, 1 tbl, 10 ex

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RU 2 320 667 C1

Authors

Maksimova Galina Vasil'Evna

Ehndjus'Kin Valerij Petrovich

Nikitina Tamara Ivanovna

Dates

2008-03-27Published

2007-01-09Filed