METHOD OF OBTAINING HIGHLY PURIFIED DIHYDROQUERCETIN Russian patent published in 2009 - IPC A61K36/00 B01D15/08 B01D15/42 

Abstract RU 2349330 C1

FIELD: chemistry.

SUBSTANCE: present invention pertains to chromatographic separation of bioflavonoids. A solution of dihydroquercetin-containing raw material in an aqueous solution of aliphatic alcohol C1-C3 is obtained. At least one chromatography cycle is carried out with depositing a sample of the obtained solution on a column, filled with hydrophobic sorbent. The mobile phase is eluted. The sample is deposited at 1-20% vol. concentration of alcohol in the solution. The mobile phase used is an aqueous solution of the same alcohol with 3% more concentration than concentration of alcohol in the solution from which the sample is deposited, but not exceeding 30% vol. The eluate obtained from chromatography is evaporated and the residue is dried.

EFFECT: obtaining high output of product with high degree of purity.

3 cl, 3 ex

Similar patents RU2349330C1

Title Year Author Number
METHOD OF OBTAINING DIHYDROQUERCETIN 2007
  • Karasev Viktor Semenovich
  • Staroverov Sergej Mikhajlovich
  • Kolesnik Jurij Arsen'Evich
  • Kolesnik Aleksej Jur'Evich
RU2349331C1
METHOD OF PRODUCING DIHYDROQUERCETIN 2010
  • Ostronkov Vladimir Sergeevich
  • Lashin Sergej Alekseevich
RU2435766C1
METHOD OF CHROMATOGRAPHIC PURIFICATION OF BUSERELIN 2007
  • Karasev Viktor Semenovich
  • Predel'Skij Andrej Dmitrievich
  • Staroverov Sergej Mikhajlovich
RU2332248C1
METHOD FOR CHROMATOGRAPHIC EXTRACTION AND PURIFICATION OF IMMUNOGLOBULINS 2018
  • Sarvin Nikita Andreevich
  • Karasev Viktor Semenovich
  • Bochkova Olga Petrovna
  • Staroverov Sergej Mikhajlovich
RU2694620C1
METHOD OF PURIFYING GOSERELIN 2015
  • Malin Aleksandr Aleksandrovich
  • Mikhajlov Oleg Rostislavovich
  • Uvarov Nikolaj Aleksandrovich
RU2578414C1
CHROMATOGRAPHIC METHOD OF EREMOMYCIN PURIFICATION 2006
  • Karasev Viktor Semenovich
  • Katrukha Genrikh Stepanovich
  • Staroverov Sergej Mikhajlovich
  • Zharov Oleg Vladimirovich
RU2333963C1
METHOD OF CHROMATOGRAPHY EXTRACTION AND CONCENTRATION OF ANTHOCYANS 2020
  • Drob Aleksandr Aleksandrovich
  • Derevyashkina Marina Evgenevna
  • Kazenina Viktoriya Vladimirovna
  • Bolshakova Ekaterina Ivanovna
  • Sarvin Nikita Andreevich
  • Vasiyarov Georgij Georgievich
  • Karasev Viktor Semenovich
  • Staroverov Sergej Mikhajlovich
RU2727130C1
METHOD FOR CHROMATOGRAPHIC EXTRACTION OF IMMUNOGLOBULIN 2010
  • Karasev Viktor Semenovich
  • Bochkova Ol'Ga Petrovna
  • Staroverov Sergej Mikhajlovich
  • Krasil'Nikov Igor' Viktorovich
  • Nikolaeva Alevtina Maksimovna
  • Petrovskikh Valentina Petrovna
  • Perevozchikov Anton Borisovich
RU2467783C2
METHOD FOR PURIFICATION OF RECOMBINANT IL-36RA (EMBODIMENTS) 2018
  • Kolobov Aleksej Aleksandrovich
  • Protasov Evgenij Aleksandrovich
  • Polotskij Aleksandr Evgenevich
  • Antipova Tatyana Olegovna
  • Sineva Svetlana Adamovna
RU2700751C1
METHOD OF PURIFYING TRIPTORELIN 2015
  • Malin Aleksandr Aleksandrovich
  • Mikhajlov Oleg Rostislavovich
  • Uvarov Nikolaj Aleksandrovich
RU2585105C1

RU 2 349 330 C1

Authors

Karasev Viktor Semenovich

Staroverov Sergej Mikhajlovich

Dates

2009-03-20Published

2007-10-15Filed