4-VINYLCYCLOHEXENE-1 SYNTHESIS METHOD Russian patent published in 2010 - IPC C07C13/20 C07C2/46 

Abstract RU 2378243 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method for synthesis of 4-vinylcyclohexene-1 through catalytic cyclodimerisation of butadiene, characterised by that, the catalyst used is Mo(CO)6 and MoO2(acac)2, the reaction is carried out in a medium of carbon tetrachloride and methanol in molar ratio [Mo]:[butadiene]:[CCl4]:[CH3OH]=1:200:200:400, at temperature 140°C for 3 hours.

EFFECT: achieving 95-100% output of end product using readily available catalyst and solvents.

1 cl, 2 ex

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RU 2 378 243 C1

Authors

Dzhemilev Usein Memetovich

Khusnutdinov Ravil Ismagilovich

Shchadneva Nina Alekseevna

Dates

2010-01-10Published

2008-08-06Filed