FIELD: chemistry.
SUBSTANCE: in the method of detecting phenol in aqueous solution via reverse-phase micro-column high-performance liquid chromatography with a preliminary sample preparation step through liquid-liquid extraction with acetonitrile, extraction is carried out at temperature 263±2 K for 30 minutes with ratio of equilibrium volume of water to the organic phase equal to 1:1.
EFFECT: simple and cheap method, high degree of extracting phenol, low detection limit.
1 ex, 3 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF DETERMINATION OF THE DIHYDROXYBENZENES IN THE WATER SOLUTIONS | 2006 |
|
RU2315994C1 |
METHOD FOR DETERMINATION OF PHENOL-TYPE ANTIOXIDANT IN VEGETABLE OIL | 2008 |
|
RU2360244C1 |
METHOD FOR DETERMINATION OF MASS CONCENTRATIONS OF PHENOL AND PYROCATECHOL IN BLOOD BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY | 2022 |
|
RU2786509C1 |
METHOD OF DETERMINING PENTAERYTHRITOL CONCENTRATION IN AQUEOUS SOLUTIONS | 2014 |
|
RU2549918C1 |
METHOD OF DETERMINING HYDROQUINONE AND PYROCATECHOL IN AQUEOUS MEDIA | 2001 |
|
RU2205398C1 |
METHOD OF DETERMINING BENZOIC ACID IN WATER | 2012 |
|
RU2529810C2 |
METHOD OF EXTRACTION OF THE VOLATILE SUBSTANCES FROM THE WATER MEDIUM | 2005 |
|
RU2296716C2 |
METHOD FOR QUANTITATIVE DETERMINATION OF ISOPROPANOL, PROPANOL AND TERT-BUTANOL IN FORMATION WATER | 2018 |
|
RU2692105C1 |
METHOD FOR DETERMINING AMOUNT OF CARMOISINE IN JUICES | 2015 |
|
RU2596796C1 |
METHOD FOR QUANTITATIVE DETERMINATION OF N-NITROSAMINES: N-DIMETHYLNITROSAMINE, N-METHYLETHYLNITROSAMINE, N-DIETHYLNITROSAMINE, N-DIBUTYLNITROSAMINE, N-DIPROPYLNITROSOAMINE, N-PIPERIDINE NITROSAMINE, N-PYRROLIDINE NITROSAMINE, N-MORPHOLIN NITROSAMINE, N-DIPHENYL NITROSAMINE, IN SAMPLES OF SMOKED MEAT PRODUCTS USING A METHOD OF CHROMATOGRAPHY-MASS SPECTROMETRY | 2017 |
|
RU2657822C1 |
Authors
Dates
2011-03-27—Published
2009-08-25—Filed