METHOD OF PRODUCING PEROVSKITES Russian patent published in 2012 - IPC C01B13/18 

Abstract RU 2440292 C2

FIELD: chemistry.

SUBSTANCE: method of producing perovskites involves mechanical mixture of initial precursor salts in stoichiometric ratio, microwave treatment of the mixture of initial salts in a microwave oven, followed by thermal treatment at temperature 500-900°C for 1-5 hours. The initial salts used for synthesis are crystalline hydrates of nitrates of rare-earth, alkali-earth and transition metals, as well as unhydrated nitrates or carbonates of the same precursors. Microwave radiation is used at operating frequency of 2.45 GHz and power of 600-1000 W for 3-10 minutes.

EFFECT: method is fast, low-waste, energy- and labour-saving and enables to obtain pure single-phase perovskites with the required characteristics, for example with a developed specific surface area or are well crystallised or thermally stable for specific regions of use.

5 cl, 4 ex, 6 tbl, 6 dwg

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RU 2 440 292 C2

Authors

Jakovleva Irina Sergeevna

Isupova Ljubov' Aleksandrovna

Dates

2012-01-20Published

2009-12-31Filed