FIELD: chemistry.
SUBSTANCE: invention discloses a method of producing 1-alkyl-2-(trimethylsilyl)cyclopropane by reacting 1-alkyl-2-(trimethylsilyl)acetylenes with triisobutylaluminium in the presence of diidomethane in an argon atmosphere at temperature 20-22°C and atmospheric pressure in dichloromethane for 3-5 hours, followed by hydrolysis of the reaction mass.
EFFECT: disclosed method enables to obtain compounds in mild conditions with high output using industrially available reagents.
1 cl, 1 tbl, 1 ex
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Authors
Dates
2012-01-20—Published
2008-12-31—Filed