METHOD OF PRODUCING 1-ALKYL-2-(TRIMETHYLSILYL)-CYCLOPROPANES Russian patent published in 2012 - IPC C07F7/08 

Abstract RU 2440360 C2

FIELD: chemistry.

SUBSTANCE: invention discloses a method of producing 1-alkyl-2-(trimethylsilyl)cyclopropane by reacting 1-alkyl-2-(trimethylsilyl)acetylenes with triisobutylaluminium in the presence of diidomethane in an argon atmosphere at temperature 20-22°C and atmospheric pressure in dichloromethane for 3-5 hours, followed by hydrolysis of the reaction mass.

EFFECT: disclosed method enables to obtain compounds in mild conditions with high output using industrially available reagents.

1 cl, 1 tbl, 1 ex

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RU 2 440 360 C2

Authors

Dzhemilev Usein Memetovich

Ramazanov Il'Fir Rifovich

Dil'Mukhametova Ljajsan Kadyrovna

Jumagulova Alsu Vakil'Evna

Sharipova Al'Fija Zufarovna

Shajbakova Marija Gennad'Evna

Dodonova Nina Egorovna

Ibragimov Askhat Gabdrakhmanovich

Sadykov Rais Askhatovich

Dates

2012-01-20Published

2008-12-31Filed