Show metadata Hide metadata

(19)

(11)

2 448 942

(13)

(51)

IPC

C07C35/37(2006-01-01)

C07C29/48(2006-01-01)

(21) (22)

Application

2010131802/04, 2010-07-28

(24)

Start date

2010-07-28

(22)

Actual filing date

2010-07-28

(45)

Published

2012-04-27

(72)

Inventor

Dzhemilev Usein MemetovichKhusnutdinov Ravil IsmagilovichShchadneva Nina AlekseevnaMajakova Julija Jur'Evna

(73)

Holder

Uchrezhdenie Rossijskoj Akademii Nauk Institut Neftekhimii I Kataliza Ran

METHOD OF PRODUCING ADAMANTANOL-1 Russian patent published in 2012 - IPC C07C35/37 C07C29/48

Abstract RU 2448942 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing adamantanol-1, which is a valuable component of lubricating oil, hydraulic and transmission fluids, as well as a starting material for production of certain drugs. The method involves reaction of adamantane with water in the medium of CCl₄ and a propionic acid amide in the presence of a vanadium catalyst VO(acac)₂ for 5-15 hours at 120-175°C in molar ratio [V]:[AdH]:[CCl₄]:[H₂O]:[CH₃CH₂CONH₂]=l:20:100:1000:100.

EFFECT: invention enables to obtain the end product with quantitative output using a simple and environmentally safe method.

1 tbl, 12 ex

Similar patents RU2448942C2

Title	Year	Author	Number
METHOD OF PRODUCING 1-HYDROXYADAMANTAN-4-ONE	2011	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Shchadneva Nina Alekseevna Majakova Julija Jur'Evna Sagitova Zilja Rashitovna	RU2491270C2
METHOD FOR PREPARING ADAMANTANOL-1	2005	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Bajguzina Al'Fija Ruslanovna Shchadneva Nina Alekseevna Burangulova Rita Junirovna Smirnov Anton Aleksandrovich	RU2286332C1
METHOD OF OBTAINING 1-HYDROXYADAMANTAN-4-ONE (KEMANTANE)	2012	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Bajguzina Al'Fija Ruslanovna Sagitova Zilja Rashitovna	RU2507191C1
METHOD OF PRODUCING 1-CHLOROADAMANTANE	2011	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Shchadneva Nina Alekseevna Oshnjakova Tat'Jana Mikhajlovna	RU2486169C2
METHOD OF OBTAINING 1-HYDROXYADAMANTHAN-4-ON	2007	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Shchadneva Nina Alekseevna Mukhametshina Lilja Fagimovna Oshnjakova Tat'Jana Mikhajlovna Atnabaeva Anna Mikhajlovna	RU2342358C2
METHOD OF PRODUCING CYCLOHEXANOL	2009	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Shchadneva Nina Alekseevna Mukhametshina Lilija Fagimovna	RU2420506C1
METHOD OF PRODUCING 1-CHLOROADAMANTYL-3-FORMAMIDE (1-CHLOROADAMANTYL-3-CARBOXYLIC ACID AMIDE)	2010	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Shchadneva Nina Alekseevna Majakova Julija Jur'Evna	RU2455282C2
PROCESS FOR PREPARING MONOCHLORO SUBSTITUTED ADAMANTANE AND DIAMANTANE DERIVATIVES	1996	Dzhemilev U.M. Khusnutdinov R.I. Shchadneva N.A. Malikov A.I.	RU2125552C1
METHOD OF PRODUCING 1-ADAMANTYLALKYL ESTERS	2012	Dzhemilev Usein Memetovich Khusnutdinov Ravil Ismagilovich Bajguzina Alfija Ruslanovna Aminov Rishat Ishbirdovich Mukminov Rinat Rifkhatovich Gimaletdinova Lejsan Ildusovna Litvinchuk Vladislav Evgenevich	RU2582620C2
METHOD OF SYNTHESIS OF 1-CHLOROADAMANTANE, 1- AND 4-CHLORODIAMANTANES	2000	Bajguzina A.R. Shchadneva N.A. Dodonova N.E. Khusnutdinov R.I. Dzhemilev U.M.	RU2185364C1

RU 2 448 942 C2

Authors

Dzhemilev Usein Memetovich

Khusnutdinov Ravil Ismagilovich

Shchadneva Nina Alekseevna

Majakova Julija Jur'Evna

Dates

2012-04-27—Published

2010-07-28—Filed