FIELD: chemistry.
SUBSTANCE: described is a method of producing 1-C1-6alkyl- and 1-phenyl-5-iodotetrazoles by reacting C1-6alkyl- and 1-phenyl-mercaptotetrazoles with hydrogen peroxide in the presence of free iodine, hydroiodic acid or hydroiodic acid salt in a solvent medium in form of acetic acid or mixture thereof with water, when the reaction is carried out using convection heating or microwave activation.
EFFECT: method is safe and environmentally friendly, and enables to significantly cut reaction time and reduce reaction temperature, which increases output of the end product, overall.
4 cl, 20 ex
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Authors
Dates
2012-12-27—Published
2011-11-01—Filed