FIELD: chemistry.
SUBSTANCE: invention relates to field of synthesis of materials used for preparation of technical and medical ceramics, as well as ion-exchangers. Method includes dissolving initial components: calcium compounds, metaphosphate, chloride in hot water. After that, obtained suspension is slowly heated to 300°C, with further heating of formed composition to 1050-1100°C. Then, it is kept at this temperature for 3-4 hours and formed fine-dispersed powder is washed with water to pH=8. As metaphosphate sodium hexametaphosphate is used.
EFFECT: method makes it possible to obtain calcium apatites with high output of target product: hydroxylapatite, chlorapatite or carbonate-substituted apatite with pure phase composition in fine-dispersed form.
2 cl, 1 tbl, 5 ex
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Authors
Dates
2013-01-27—Published
2011-02-08—Filed