METHOD OF PRODUCING (E)-4-PHENYL-3-BUTEN-2-ONE Russian patent published in 2013 - IPC C07C49/217 C07C45/69 C07C45/65 

Abstract RU 2481321 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing (E)-4-phenyl-3-buten-2-one (benzalacetone) which can be used as a taste and aroma additive in the food industry and perfumery. The method involves reaction of styrene and acetic anhydride in the presence of a mesoporous amorphous aluminium-silicon-zircon oxide catalyst in molar ratio styrene:acetic anhydride=1:2-8, at temperature of 80-130°C, weight content of catalyst of 10-50% (with respect to the mixture of styrene and acetic anhydride, taken in molar ratio of 1:1).

EFFECT: invention enables to obtain the end product using a simple and low-cost method.

8 ex, 1 tbl

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RU 2 481 321 C1

Authors

Dzhemilev Usein Memetovich

Kutepov Boris Ivanovich

Grigor'Eva Nellja Gennad'Evna

Veklov Vitalij Aleksandrovich

Sulejmanova Ajgul' Mukhamatovna

Jamali Elena Ivanovna

Dates

2013-05-10Published

2011-11-24Filed