FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing (E)-4-phenyl-3-buten-2-one (benzalacetone) which can be used as a taste and aroma additive in the food industry and perfumery. The method involves reaction of styrene and acetic anhydride in the presence of a mesoporous amorphous aluminium-silicon-zircon oxide catalyst in molar ratio styrene:acetic anhydride=1:2-8, at temperature of 80-130°C, weight content of catalyst of 10-50% (with respect to the mixture of styrene and acetic anhydride, taken in molar ratio of 1:1).
EFFECT: invention enables to obtain the end product using a simple and low-cost method.
8 ex, 1 tbl
Title | Year | Author | Number |
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METHOD OF PRODUCING (E)-4-PHENYL-3-BUTEN-2-ONE | 2011 |
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METHOD OF PRODUCING MESOPOROUS AMORPHOUS COMPOSITE ELEMENTOSILICATES | 2009 |
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RU2759627C2 |
METHOD OF PRODUCING 2,2,4-TRIALKYL-2,3-DIHYDRO-1H-1,5-BENZODIAZEPINES | 2019 |
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Authors
Dates
2013-05-10—Published
2011-11-24—Filed