METHOD OF PRODUCING 2-METHYL-3-PROPYLINDOLE Russian patent published in 2024 - IPC C07D209/08 

Abstract RU 2831365 C1

FIELD: chemistry.

SUBSTANCE: invention relates to organic chemistry, specifically to a method of producing 2-methyl-3-propylindole, which can be used as a repellent in marine antifouling material against living organisms, for synthesis of indole derivatives and photochromic dyes. Method is characterized by that 2-methyl-3-propylindole is obtained by reacting aniline with 1,2-propanediol in the presence of granular zeolite Yh in H-form with a hierarchical porous structure, in autoclave at 260 °C, molar ratio of aniline : 1,2-propanediol = 1:2-5, in presence of 5-20 wt.% catalyst H-Yh, for 6-9 hours.

EFFECT: simplification of heterogeneous catalytic synthesis of end product from available and safe raw material.

1 cl, 1 tbl, 6 ex

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Authors

Boris Ivanovich Kutepov

Nellia Gennadevna Grigoreva

Anna Sergeevna Artemeva

Sergei Vladimirovich Bubennov

Vera Rafaelevna Bikbaeva

Nadezhda Aleksandrovna Filippova

Dates

2024-12-04Published

2024-05-07Filed