FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing (E)-4-phenyl-3-buten-2-one (benzalacetone) (I) 
which can be used as a taste and aroma additive in the food industry and perfumery. The method involves reaction of styrene and acetic anhydride in the presence of zeolite Beta in H-form at temperature of 80-130°C, catalyst amount of 10-50 wt % (with respect to the mixture of styrene and acetic anhydride, taken in molar ratio of 1:1) and molar ratio of styrene to acetic anhydride of 1:2-8.
EFFECT: invention enables to obtain the end product using a simple and low-cost method as well as readily available reactants.
7 ex, 1 tbl
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING (E)-4-PHENYL-3-BUTEN-2-ONE | 2011 |
|
RU2482105C1 |
| METHOD OF PRODUCING (E)-4-PHENYL-3-BUTEN-2-ONE | 2011 |
|
RU2481321C1 |
| METHOD OF PRODUCING 1-ISOALKOXY-1-PHENYLETHANES | 2008 |
|
RU2404958C2 |
| METHOD OF PRODUCING CYCLIC HOMO- AND CO-DIMERS OF STYRENE AND ALPHA-METHYLSTYRENE | 2010 |
|
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| METHOD OF PRODUCING 2-METHYL-3-PROPYLINDOLE | 2024 |
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| METHOD FOR OBTAINING 2-ETHYL-3,5-DIMETHYL PYRIDINE | 2016 |
|
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| METHOD OF PRODUCING HOMO- AND CO-OLIGOMERS OF Α-METHYLSTYRENE AND ISOPENTENES IN THE PRESENCE OF HIERARCHICAL ZEOLITE H-YMMM | 2020 |
|
RU2735666C1 |
| METHOD OF PRODUCING 3,4-DIMETHYL-1-PHENYLPYRROLE | 2023 |
|
RU2830162C1 |
| METHOD OF PRODUCING 1-ALKOXY-1-PHENYLETHANES | 2008 |
|
RU2404957C2 |
| METHOD FOR COMBINED SYNTHESIS OF LINEAR CYCLIC HOMO- AND CODIMERS OF STYRENE AND α-METHYLSTYRENE | 2010 |
|
RU2424221C1 |
