METHOD OF PRODUCING ISOTOPICALLY-ENRICHED GERMANIUM Russian patent published in 2013 - IPC C22B41/00 

Abstract RU 2483130 C1

FIELD: metallurgy.

SUBSTANCE: proposed method comprises plasma chemical decomposition of isotopically-enriched germanium in the mix with hydrogen in nonequilibrium plasma of HF discharge and depositing germanium on substrate. Note here that said deposition is performed outside the discharge fire zone at the pressure of 200-300 mTorr, GeF4-to-H2 ratio making at least 1:4 and their total flow rate of 100-150 cm3/min. Output of this method makes at least 5 g/h of polycrystalline germanium with yield of finished product making 90-95% which allows growing monocrystals of isotopically-enriched germanium of good quality in amount of, at least, several tens of grams.

EFFECT: higher efficiency and yield.

1 ex, 1 tbl

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RU 2 483 130 C1

Authors

Sennikov Petr Gennad'Evich

Golubev Sergej Vladimirovich

Shashkin Vladimir Ivanovich

Koldanov Vladimir Aleksandrovich

Prjakhin Dmitrij Aleksandrovich

Kornev Roman Alekseevich

Mochalov Leonid Aleksandrovich

Zyrjanov Sergej Mikhajlovich

Filimonov Sergej Vasil'Evich

Rogozhin Dmitrij Viktorovich

Dates

2013-05-27Published

2011-11-24Filed