FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing a complex of copper with 5,5-dimethyl-1,3-cyclohexanedione of formula CuL2, where L is 5,5-dimethyl-1,3-cyclohexanedione. The method involves preparation of a solution of 5,5-dimethyl-1,3-cyclohexanedione and lithium chloride in ethyl alcohol in ratio of 5:0.5:100, electrolysis of the obtained solution with copper electrodes, separating the obtained precipitate, washing the precipitate and drying the precipitate. Electrolysis is carried out using pulsed electric current with pulse duration of 5 s and current density of 2-4 mA/cm2.
EFFECT: invention enables to obtain said complex, which can be used to make high-temperature superconductors, catalysts and stabilisers.
3 tbl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD FOR OBTAINING COORDINATION COMPOUND OF COPPER(II) WITH NICOTINIC ACID | 2017 |
|
RU2647072C1 |
| METHOD FOR OBTAINING COORDINATION COMPOUND OF COPPER(II) WITH PICOLINIC ACID | 2017 |
|
RU2654464C1 |
| METHOD OF OBTAINING COORDINATION COMPOUNDS Er(III) AND Yb(III) WITH 5,5-DIMETHYL-1,3-CYCLOHEXANDIONE | 2007 |
|
RU2343156C1 |
| METHOD FOR PRODUCING A COORDINATION COMPOUND OF COPPER(II) WITH 2,3,4,5-TETRAHYDRO-2-IMINO-4-OXO-1,3-THIAZOLE-5-ACETIC ACID | 2021 |
|
RU2774950C1 |
| METHOD OF PREPARING DISSIMILAR-LIGAND COMPLEXES OF RARE-EARTH ELEMENTS WITH ACETYLACETONE AND CIS- OR TRANS-BUTEDIOIC ACID | 2002 |
|
RU2237749C2 |
| METHOD FOR PRODUCTION OF COPPER (II) AND ZINC (II) ACETYLACETONATES | 2005 |
|
RU2281935C1 |
| METHOD OF PRODUCING COORDINATION COMPOUND OF COPPER(II) WITH 1,10-PHENANTHROLINE AND DL-TRYPTOPHAN | 2014 |
|
RU2584007C1 |
| METHOD OF PRODUCING COMPLEX COMPOUND OF COPPER AND PYRIDOXINE | 2009 |
|
RU2415860C1 |
| METHOD OF PRODUCING TETRA-1,10-PHENANTHROLINE-μ-FUMARATE-DICOOPER(II) CHLORIDE | 2019 |
|
RU2702119C1 |
| METHOD OF OBTAINING THE COORDINATION CONNECTION OF ZINC WITH NICOTINE ACID | 2016 |
|
RU2618533C1 |
