FIELD: physics.
SUBSTANCE: new type of silica planar plates with binding is developed for separation of isomers of optically active compounds which contains the macrocyclic glycopeptide antibiotic eremomicyn as a chiral selector. The method of immobilization of eremomicyn by superficial assembly which consists in that silicon dioxide with inorganic binding in a water buffer solution is treated first by γ-glycide hydroxi propyl trialkoxysilane, and then in alkaline water solution to silicon dioxide and inorganic binding (salt of silicon acid), modified by epoxy groups, the macrocyclic glycopeptide antibiotic eremomicyn is intergrafted.
EFFECT: obtaining of high efficient chiral planar plates for thin layer chromatography with high value of enantioselectivity.
3 tbl, 1 dwg
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF OBTAINING THIN-LAYER CHIRAL PLATES FOR PLANAR CHROMATOGRAPHY OF STEREOISOMERS AND THEIR RACEMIC MIXTURES | 2013 |
|
RU2541524C2 |
| SORBENT FOR RESOLUTION OF OPTICAL ISOMERS AND A METHOD FOR PREPARATION THEREOF | 2004 |
|
RU2255802C1 |
| SORBENT FOR OPTIC ISOMER CHROMATOGRAPHY AND METHOD OF ITS OBTAINMENT | 2006 |
|
RU2348455C2 |
| METHOD FOR PREPARATION OF ENANTIOSELECTIVE SORBENT | 2008 |
|
RU2363538C1 |
| SORBENT FOR SEPARATION OF OPTICAL ISOMERS OF SUBSTANCES AND ANALYSIS THEREOF IN BIOLOGICAL FLUIDS BY HPLC AND PREPARATION METHOD THEREOF | 2014 |
|
RU2592893C2 |
| METHOD FOR SELECTIVE SEPARATION OF SALBUTAMOL RACEMIC MIXTURE | 2017 |
|
RU2667002C1 |
| METHOD OF CHIRAL SORBENTS PRODUCTION | 2007 |
|
RU2339445C1 |
| METHOD OF SEPARATING AND DETECTING AMINO ACIDS | 1994 |
|
RU2095808C1 |
| METHOD OF SEPARATING AMINO ACIDS IN BODY FLUIDS | 1993 |
|
RU2078342C1 |
| SORBENT AND METHOD OF PREPARATION THEREOF | 2001 |
|
RU2203730C1 |
