FIELD: chemistry.
SUBSTANCE: invention relates to analytical chemistry for element analysis and can be used for laser-spark emission determination of lanthanum, cerium, praseodymium and neodymium in metal alloys and powders. The method is based on exposing the surface of an analysed sample to focused laser radiation with pulse energy of 0.12-0.9 J and pulse duration of 0.02-240 mcs. Laser spark luminescence analysis is carried out, which enables to pick out spectral lines of the vapour of the determined elements and identify spectral lines. Each of the elements is determined using experimentally determined most sensitive laser emission lines of elements in the following ranges: lanthanum 390-415 nm, cerium 400-425 nm, praseodymium 410-425 nm, neodymium 400-415 nm.
EFFECT: performing laser-spark emission determination of lanthanum, cerium, praseodymium and neodymium in metal alloys and powders.
Title | Year | Author | Number |
---|---|---|---|
METHOD OF LASER-SPARK EMISSION DETERMINATION OF ARSENIC IN FOOD RAW MATERIAL AND FOODSTUFF | 2013 |
|
RU2531026C1 |
METHOD FOR LASER-SPARK EMISSION DETERMINATION OF TOXIC ELEMENTS IN FOOD RAW MATERIAL AND PRODUCTS | 2011 |
|
RU2483294C2 |
METHOD FOR LASER-SPARK EMISSION DETERMINATION OF BERYLLIUM IN METAL ALLOYS AND POWDERS | 2015 |
|
RU2583858C1 |
LASER-SPARK SPECTRUM ANALYZER | 2000 |
|
RU2163370C1 |
MARKING ADDITIVE FOR EXPLOSIVE SUBSTANCE, METHOD OF PREPARATION THEREOF, METHOD OF DETERMINING ORIGIN OF EXPLOSIVE SUBSTANCE, AND DEVICE TO IMPLEMENT IT | 2005 |
|
RU2283823C1 |
METHOD OF DETERMINING CONCENTRATION OF RARE-EARTH ELEMENTS: LANTHANUM, CERIUM, PRASEODYMIUM, NEODYMIUM, SAMARIUM, EUROPIUM, GADOLINIUM, TERBIUM, DYSPROSIUM, HOLMIUM, ERBIUM, THULIUM, YTTERBIUM, LUTETIUM AND YTTRIUM, IN AIR OF THE WORKING ZONE BY MASS SPECTROMETRY WITH INDUCTIVELY COUPLED PLASMA | 2018 |
|
RU2697479C1 |
METHOD OF DETERMINING WEIGHT RATIO OF OXYGEN IN METAL POWDERS | 2013 |
|
RU2530483C1 |
MOBILE LASER EMISSION SUBSTANCE ANALYSER | 2020 |
|
RU2751434C1 |
METHOD OF DETERMINING BLOOD CONTENT OF RARE-EARTH ELEMENTS: YTTRIUM, LANTHANUM, CERIUM, PRASEODYMIUM, NEODYMIUM, SAMARIUM, EUROPIUM, GADOLINIUM, TERBIUM, DYSPROSIUM, HOLMIUM, ERBIUM, THULIUM, YTTERBIUM AND LUTETIUM BY MASS SPECTROMETRY WITH INDUCTIVELY COUPLED PLASMA | 2019 |
|
RU2696011C1 |
COMPOSITE CATHODE MATERIAL PRODUCTION TECHNIQUE | 2016 |
|
RU2639719C1 |
Authors
Dates
2015-04-20—Published
2013-09-04—Filed