FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing (1,5,3-dithiazepan-3-yl)-alkanediols. The method includes reacting bis(methoxymethyl)aminoalkanediol (bis(methoxymethyl)-2-aminopropane-1,3-diol; bis(methoxymethyl)-2-amino-2-methylpropane-1,3-diol; bis(methoxymethyl)-3-aminopropane-1,2-diol) with 1,2-ethanedithiol in the presence of a SmCl3·6H2O catalyst in the medium of methanol-chloroform solvents at room temperature for 2.5-3.5 hours. Output of (1,5,3-dithiazepan-3-yl)-alkanediols (1) is 50-63%.
EFFECT: compounds can be used as antimicrobial, antifungal and anti-inflammatory agents, as well selective complexing agents and biocides.
1 tbl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING (1,5,3-DITHIAZEPAN-3-YL)-ALKANEDIOLS | 2013 |
|
RU2559359C2 |
| METHOD OF PRODUCING N-CYCLOALKYL-SUBSTITUTED 1,5,3-DITHIAZEPANES | 2015 |
|
RU2601313C1 |
| METHOD OF PRODUCING OF BIS-(1,5,3-DITHIAZEPAN-3-IL)CYCLOHEXANES | 2014 |
|
RU2574069C1 |
| METHOD OF PRODUCING N-CYCLOPENTYL-SUBSTITUTED 1,5,3-DITHIAZEPANES | 2014 |
|
RU2565790C1 |
| METHOD FOR OBTAINING N-CYCLOALKYL SUBSTITUTED 1,5,3-DITHIAZEPANES | 2017 |
|
RU2664654C2 |
| METHOD OF PRODUCING N,N-BIS-[(1,5,3-DITHIAZEPAN-3-YL)ALKYL]AMINES | 2014 |
|
RU2591196C2 |
| METHOD OF PRODUCING METHYL 2-(1,5,3-DITHIAZEPAN-3-YL)ALKANOATES | 2015 |
|
RU2605448C1 |
| METHOD OF PRODUCING N-ADAMANTYL-1,5,3-DITHIAZEPANES | 2015 |
|
RU2605447C1 |
| METHOD OF PRODUCING 3-[1-(1-ADAMANTYL)ETHYL]-1,5,3-DITHIAZEPANE AND USE THEREOF AS FUNGICIDALLY ACTIVE AGENT | 2014 |
|
RU2574292C1 |
| METHOD OF PRODUCING 3-(1-ADAMANTYL)-1,5,3-DITIAZEPANE AND USE THEREOF AS FUNGICIDALLY ACTIVE AGENT | 2014 |
|
RU2584692C2 |
