FIELD: chemistry.
SUBSTANCE: method for sulfating xylan birch wood with chlorosulfonic acid in an organic solvent is characterized in that the sulfation is carried out in 1,4-dioxane at a temperature of 20-40°C for 3-6 hours, and xylan sulfate is isolated after neutralisation of the reaction mass with a 3% aqueous solution of sodium hydroxide, followed by purification by dialysis.
EFFECT: effective way of sulphating xylan.
1 tbl, 9 ex
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Authors
Dates
2017-05-29—Published
2016-06-22—Filed