METHOD FOR PREPARING DIALKYLNORBORNENE-2,3-DICARBOXYLATES Russian patent published in 2017 - IPC C07C69/753 C07C67/347 

Abstract RU 2625788 C1

FIELD: chemistry.

SUBSTANCE: method for preparing dialkylnorbornene-2.3-dicarboxylates is carried out by reacting dialkyl diester of fumaric acid with cyclopentadiene (CPD), as a source of CPD, C5 fraction of pyrolysis is used in an amount providing a molar ratio of alkyl diester of fumaric acid and CPD of 1:1.5-3.0, wherein C5 fraction is dosed into the alkyl diester of fumaric acid at a reaction mass of 16-20°C. The reaction is then carried out at room temperature until the fumaric acid diester is completely consumed, after which the excess of C5 fraction is distilled off at a temperature of 30-60°C and at an atmospheric pressure, and the bottom residue is evacuated at a pressure of 2-10 mm Hg and at the temperature in the cube of 50-80°C.

EFFECT: expanding raw material sources, simplifying the method, reducing the cost price.

2 cl, 2 tbl, 6 ex

Similar patents RU2625788C1

Title Year Author Number
METHOD OF PRODUCING AN NAPHTHALATE MIXTURE PLASTICIZER 2018
  • Lakeev Sergej Nikolaevich
  • Ganeev Artur Elvirovich
  • Shcherbakov Vasilij Vasilevich
  • Ishalina Olga Vladimirovna
RU2691739C1
METHOD FOR SELECTIVE PREPARATION OF EXO,EXO- AND ENDO,ENDO-DI(2-ETHYLHEXYL)NORBORNENE-2,3-DICARBOXYLATES FROM C5 FRACTION OF LIQUID PYROLYSIS PRODUCTS 2020
  • Lakeev Sergei Nikolaevich
RU2754913C1
METHOD OF PRODUCING ESTER PLASTICISER 2018
  • Lakeev Sergej Nikolaevich
  • Shcherbakov Vasilij Vasilevich
  • Minnigulov Raif Zulfatovich
  • Ishalina Olga Vladimirovna
RU2696261C1
METHOD OF PRODUCING CITRATED PLASTICISER 2019
  • Lakeev Sergej Nikolaevich
  • Shcherbakov Vasilij Vasilevich
RU2699018C1
METHOD OF PRODUCING NEW BENZOATE PLASTICISER 2019
  • Lakeev Sergej Nikolaevich
  • Shcherbakov Vasilij Vasilevich
RU2699016C1
METHOD OF PRODUCING TEREPHTHALATE AND BENZOATE PLASTICIZERS FROM BY-PRODUCTS 2019
  • Lakeev Sergej Nikolaevich
  • Shcherbakov Vasilij Vasilevich
RU2708641C1
METHOD OF PREPARING ASYMMETRIC ESTER BASE OF SYNTHETIC LUBRICATING OIL 0
  • Belov Petr Stepanovich
  • Zavorotnyj Viktor Aleksandrovich
  • Korenev Konstantin Dmitrievich
  • Lashkhi Konstantin Dmitrievich
  • Vipper Andrej Borisovich
  • Ermolov Fridrikh Nikolaevich
  • Kulagin Vladimir Vasilevich
  • Tsvetkov Oleg Nikolaevich
SU709617A1
METHOD FOR CONTINUOUS PRODUCTION OF LIGHT COOLIGOPIPERYLENE POLYMERIC PETROLEUM RESIN 2011
  • Popov Boleslav Ivanovich
  • Lakeev Sergej Nikolaevich
  • Liakumovich Aleksandr Grigor'Evich
RU2473569C1
PLASTICISER FOR POLYVINYL CHLORIDE COMPOSITIONS 2009
  • Lakeev Sergej Nikolaevich
  • Karchevskij Stanislav Gennadievich
RU2404156C1
METHOD FOR OBTAINING CARBOXYLIC ACID ESTERS IN PRESENCE OF TITANIUM-CONTAINING CATALYST 2014
  • Kolesnik Vasilij Dmitrievich
  • Nosikov Aleksej Aleksandrovich
  • Kalinin Rodion Georgievich
  • Bobrikova Anastasiya Aleksandrovna
  • Sherstobitov Ivan Anatolevich
RU2656338C1

RU 2 625 788 C1

Authors

Lakeev Sergej Nikolaevich

Valeev Ruslan Faridovich

Ganeev Artur Elvirovich

Dates

2017-07-19Published

2016-11-02Filed